四丁基溴化磷

15篇引用文献

≥98%

CAS编号: 3115-68-2
分子式: C₁₆H₃₆BrP
分子量: 339.33
Beilstein号: 4160474
EC号: 221-487-8
MDL号: MFCD00011853
PubChem编号: 76564

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货号 (SKU)	包装规格	是否现货
T107471-5g	5g	现货
T107471-25g	25g	现货
T107471-100g	100g	现货
T107471-500g	500g	现货
T107471-1kg	1kg	现货

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基本描述

别名	四丁基溴化膦 \| 四丁基溴化鏻
英文别名	2953275L2K \| CAS-3115-68-2 \| MFCD00011853 \| Tetra- n -butylphosphonium Bromide ( TBPB ) \| N,N,N',N'-Tetramethyltetramethylenediamine \| Tox21_200701 \| SCHEMBL126636 \| tetrabutylphosphanium bromide \| UNII-2953275L2K \| A820742 \| PX 4B \| Q27254381 \| AS-12267
规格或纯度	≥98%
英文名称	Tetrabutylphosphonium bromide
应用	A useful synthetic reagent used in proteomics research. Tetrabutylphosphonium bromide (TBPB) is a quaternary salt which can be used: · As a medium to disperse ruthenium catalyst for the synthesis of ethylene glycol from synthesis gas via ruthenium melt catalysis. · As a catalyst supported on silica or alumina for the halogen exchange reaction to synthesize alkyl bromide from alkyl chloride. · To synthesize various ionic liquids on mixing with different proportions of 1,3-dimethylurea for capturing NO gas. · As a hydrogen-bond acceptor along with levulinic acid as a hydrogen-bond donor for the preparation of deep eutectic solvents to separate toluene from toluene/n-hexane mixtures. · To prepare ionic semiclathrate hydrates
储存温度	充氩
运输条件	常规运输
产品介绍	溶解度：70%水、20%甲醇、80%2-丙醇、50%甲苯。A useful synthetic reagent used in proteomics research. Tetrabutylphosphonium bromide (TBPB) is a quaternary salt which can be used: · As a medium to disperse ruthenium catalyst for the synthesis of ethylene glycol from synthesis gas via ruthenium melt catalysis. · As a catalyst supported on silica or alumina for the halogen exchange reaction to synthesize alkyl bromide from alkyl chloride. · To synthesize various ionic liquids on mixing with different proportions of 1,3-dimethylurea for capturing NO gas. · As a hydrogen-bond acceptor along with levulinic acid as a hydrogen-bond donor for the preparation of deep eutectic solvents to separate toluene from toluene/n-hexane mixtures. · To prepare ionic semiclathrate hydrates A useful synthetic reagent used in proteomics research.

名称和识别符

EC号	221-487-8
分子类型	小分子
IUPAC Name	tetrabutylphosphanium;bromide
INCHI	InChI=1S/C16H36P.BrH/c1-5-9-13-17(14-10-6-2,15-11-7-3)16-12-8-4;/h5-16H2,1-4H3;1H/q+1;/p-1
InChi Key	RKHXQBLJXBGEKF-UHFFFAOYSA-M
Canonical SMILES	CCCC[P+](CCCC)(CCCC)CCCC.[Br-]
Isomeric SMILES	CCCC[P+](CCCC)(CCCC)CCCC.[Br-]
WGK Germany	1
RTECS	TA2417000
PubChem CID	76564
UN Number	3464
分子量	339.33
Beilstein号	4160474
Reaxy-Rn	4160474

化学和物理性质

溶解性	Soluble in water (70 g/100 ml)
敏感性	对热、光敏感，易吸潮
闪点(℉)	554 °F
闪点(℃)	290°C
熔点	99-103°C
分子量	339.330 g/mol
XLogP3
氢键供体数Hydrogen Bond Donor Count	0
氢键受体数Hydrogen Bond Acceptor Count	1
可旋转键计数Rotatable Bond Count	12
精确质量Exact Mass	338.174 Da
单同位素质量Monoisotopic Mass	338.174 Da
拓扑极表面积Topological Polar Surface Area	0.000 Å²
重原子数Heavy Atom Count	18
形式电荷Formal Charge	0
复杂度Complexity	116.000
同位素原子数Isotope Atom Count	0
定义的原子立体中心计数Defined Atom Stereocenter Count	0
未定义的原子立体中心计数Undefined Atom Stereocenter Count	0
定义的键立体中心计数Defined Bond Stereocenter Count	0
未定义的键立体中心计数Undefined Bond Stereocenter Count	0
所有立体化学键的总数The total count of all stereochemical bonds	0
共价键合单元计数Covalently-Bonded Unit Count	2

安全和危险性（GHS）

象形图	GHS06, GHS09, GHS05, GHS07
信号词	Danger
危险声明	H315: 引起皮肤刺激 H319: 引起严重眼睛刺激 H335: 可能引起呼吸道刺激 H311: 皮肤接触有毒 H411: 对水生生物有毒并具有长期持续影响 H302: 吞食有害 H318: 造成严重的眼睛损伤 H310: 与皮肤接触致命
预防措施声明	P261: 避免吸入灰尘/烟雾/气体/雾/蒸汽/喷雾 P305+P351+P338: 如进入眼睛：用水小心冲洗几分钟。如戴隐形眼镜并可方便地取出，取出隐形眼镜。继续冲洗。 P273: 避免释放到环境中。 P280: 戴防护手套/穿防护服/戴防护眼罩/戴防护面具。 P302+P352: 如皮肤沾染：用水充分清洗。 P321: 特殊处理（请参阅此标签上的...）。 P405: 密闭存放 P501: 将内容物/容器处理到。。。 P264: 处理后要彻底洗手。 P271: 仅在室外或通风良好的地方使用。 P270: 使用本产品时，请勿进食、饮水或吸烟。 P304+P340: 如误吸入：将人转移到空气新鲜处，保持呼吸舒适体位。 P403+P233: 存放在通风良好的地方。保持容器密闭。 P362+P364: 脱掉沾污的衣服，清洗后方可重新使用。 P391: 收集溢出物 P330: 漱口 P262: 不要进入眼睛、皮肤或衣服。 P361+P364: 立即脱掉所有沾染的衣服，清洗后方可重新使用。 P264+P265: 处理后彻底洗手[和…]。不要触摸眼睛。 P301+P317: 如果被吞咽：请寻求医疗帮助。 P305+P354+P338: 如果进入眼睛：立即用水冲洗几分钟。取下隐形眼镜（如果有的话），并且操作简单。继续冲洗。 P317: 寻求紧急医疗救助。 P337+P317: 如果眼睛刺激持续：寻求医疗帮助。 P332+P317: 如果出现皮肤刺激：请寻求医疗帮助。 P316: 立即寻求紧急医疗救助。 P319: 如果你感到不适，请寻求医疗帮助。
WGK Germany	1
RTECS	TA2417000
Reaxy-Rn	4160474
个人防护装备	dust mask type N95 (US)， Eyeshields， Faceshields， full-face particle respirator type N100 (US)， Gloves， respirator cartridge type N100 (US)， type P1 (EN143) respirator filter， type P3 (EN 143) respirator cartridges

SDS英文版

技术规格说明书

Purity(Titration by AgNO3)	97.5-102.5（%）
Melting point	99-106（℃）
Appearance（T107471)	White to Off-White Powder or Crystals
Infrared spectrum	Conforms to Structure
Solubility in H2O	Almost transparency

技术规格说明书

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找到13个结果

批号(Lot Number)	证书类型	日期	货号
H2522098	分析证书	25-09-03	T107471
G2303219	分析证书	25-04-14	T107471
G2303221	分析证书	25-04-14	T107471
G2303222	分析证书	25-04-14	T107471
G2510066	分析证书	25-04-14	T107471
A2509055	分析证书	23-06-26	T107471
G2303218	分析证书	23-06-26	T107471
G2303220	分析证书	23-06-26	T107471
G2411024	分析证书	23-06-26	T107471
J2424010	分析证书	23-06-26	T107471
L2418017	分析证书	23-06-26	T107471
B2310605	分析证书	22-11-11	T107471
K2210248	分析证书	22-11-11	T107471

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1. Haolin Li, Fan Xu, Kun Cui, Bingyu Tian, Rui Dong, Mingjin Fan. (2023) Interfacial adsorption and tribological response of various functional groups on titanium surface: In-depth research conducted on the lubricating mechanism of liquid lubricants. TRIBOLOGY INTERNATIONAL, 189 (108885). [10.1016/j.triboint.2023.108885]
2. Hongye Cheng, Guojin Zhang, Yaxi Zhang, Zhen Song, Zhiwen Qi. (2023) Solute structure effect on aromatics-alkanes extractive separation toward rational LCO upgrading. SEPARATION AND PURIFICATION TECHNOLOGY, 310 (123213). [10.1016/j.seppur.2023.123213]
3. Zhenyu Lu, Yufei Hu, Gongke Li, Ling Xia. (2022) Adamantane Three-Dimensional Porous Organic Framework as a Fluorescence Sensor for Rapid Determination of Tetracycline in Aquatic Products. Chemosensors, 10 (11): (457). [10.3390/chemosensors10110457]
4. Xueshan Sun, Xuezhen Wang, Yingli Wan, Yafei Guo, Tianlong Deng, Xiaoping Yu. (2023) Synthesis of functional ionic liquids with high extraction rate and electroconductivity for lithium-magnesium separation and metallic magnesium production from salt lake brine. CHEMICAL ENGINEERING JOURNAL, 452 (139610). [10.1016/j.cej.2022.139610]
5. Haolin Li, Lin Ma, Ping Wen, Yunyan Han, Rui Dong, Mingjin Fan. (2022) Molecular structure insight into the tribological behavior of sulfonate ionic liquids as lubricants for titanium alloys. JOURNAL OF MOLECULAR LIQUIDS, 357 (119082). [10.1016/j.molliq.2022.119082]
6. Zhen Ge, Hongye Cheng, Guojin Zhang, Linsheng Wang, Zhiwen Qi. (2022) Mechanism of Extractive Separation of Light Cycle Oil Using a Deep Eutectic Solvent Composed of Tetrabutylphosphonium Bromide and Levulinic Acid. ENERGY & FUELS, 36 (4): (1854–1862). [10.1021/acs.energyfuels.1c03856]
7. Yan Wang, Dong-Liang Zhong, Peter Englezos, Jin Yan, Bin-Bin Ge. (2020) Kinetic study of semiclathrate hydrates formed with CO2 in the presence of tetra-n-butyl ammonium bromide and tetra-n-butyl phosphonium bromide. ENERGY, 212 (118697). [10.1016/j.energy.2020.118697]
8. Zhiming Wu, Qian Zeng, Hongye Cheng, Lifang Chen, Zhiwen Qi. (2020) Extractive separation of tetralin-dodecane mixture using tetrabutylphosphonium bromide-based deep eutectic solvent. Chemical Engineering and Processing-Process Intensification, 149 (107822). [10.1016/j.cep.2020.107822]
9. Hongtao Cai, Ran Kou, Guangming Liu. (2019) Counterion-Tunable Thermosensitivity of Strong Polyelectrolyte Brushes. LANGMUIR, 35 (51): (16862–16868). [PMID:31774295] [10.1021/acs.langmuir.9b02982]
10. Yu-Mei Liu, Yan Zhou, Wen-Qiang Gong, Zhang-Min Li, Chao-Li Wang, Duan-Jian Tao. (2020) Highly efficient synthesis of 1-methoxy-2-propanol using ionic liquid catalysts in a micro-tubular circulating reactor. Green Energy & Environment, 5 (147). [10.1016/j.gee.2019.09.001]
11. Lei Liu, Xinyu Fu, Hongliang Zhang, Weiqing Ma, Lili Zhang, Yixin Zhang, Meng Liu, Kehan Liang, Senlin Hou, Aibing Chen. (2018) Luminogen-functionalized mesoporous SBA-15 for fluorescent detection of antibiotic cefalexin. JOURNAL OF MATERIALS RESEARCH, 33 (10): (1442-1448). [10.1557/jmr.2018.96]
12. Yalan Dai, Peiyi Wu. (2017) Toward the two-step microdynamic phase transition mechanism of an oligo(ethylene glycol)methacrylate-based copolymer with a LCST-type poly(ionic liquid) block. PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 19 (28): (18556-18564). [PMID:28686277] [10.1039/C7CP02942J]
13. Ge Wang, Peiyi Wu. (2016) Unusual Phase Transition Behavior of Poly(N-isopropylacrylamide)-co-Poly(tetrabutylphosphonium styrenesulfonate) in Water: Mild and Linear Changes in the Poly(N-isopropylacrylamide) Part. LANGMUIR, 32 (15): (3728–3736). [PMID:27022971] [10.1021/acs.langmuir.6b00392]
14. Ouyang Fan, Zhou Yan, Li Zhang-Min, Hu Na, Tao Duan-Jian. (2014) Tetrabutylphosphonium amino acid ionic liquids as efficient catalysts for solvent-free Knoevenagel condensation reactions. KOREAN JOURNAL OF CHEMICAL ENGINEERING, 31 (8): (1377-1383). [10.1007/s11814-014-0077-4]
15. Duan-Jian Tao, Fan Ouyang, Zhang-Min Li, Na Hu, Zhen Yang, Xiang-Shu Chen. (2013) Synthesis of Tetrabutylphosphonium Carboxylate Ionic Liquids and Its Catalytic Activities for the Alcoholysis Reaction of Propylene Oxide. INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 52 (48): (17111–17116). [10.1021/ie402250e]
16. Jing Fan, Xin Zhang, Nan He, Fenhong Song, Hongwei Qu. (2024) Deep Eutectic Solvent + Water System in Carbon Dioxide Absorption. MOLECULES, 29 (15): (3579). [PMID:39124983] [10.3390/molecules29153579]
17. Nan He, Yukun Zhang, Fenhong Song, Jing Fan, Xiwu Zhang. (2025) Experimental and theoretical investigation of CO2 solubility in amine-based deep eutectic solvents. FLUID PHASE EQUILIBRIA, 587 (114203). [10.1016/j.fluid.2024.114203]
18. Jie Wang, Jielin Huang, Hui Xu, Li Dong, Songsong Chen, Junping Zhang, Suojiang Zhang. (2024) Phosphorus-modulated surface active center reconstruction in cerium oxide for polyols conversion into carbonates. APPLIED CATALYSIS B-ENVIRONMENTAL, 357 (124284). [10.1016/j.apcatb.2024.124284]
19. Lijiao Yu, Lihong Deng, Jieyu Wu, Subhan Mahmood, Ke Yuan, Haoran Wu, Xiaodong Wang, Jing Zhang, Shun Yao. (2025) Purification of crude tea tree oil through enrichment of terpinen-4-ol by in-situ formation of deep eutectic solvent. SEPARATION AND PURIFICATION TECHNOLOGY, 362 (131806). [10.1016/j.seppur.2025.131806]
20. Bao Ke, Hui Peng, Yongqi Yang, Chengzhi Yang, Shangfei Yao, Arfan Bukhtiar, Qilin Wei, Jialong Zhao, Bingsuo Zou. (2024) Realizing efficient broadband near-infrared emission under blue light excitation in Sb3+-doped zero-dimensional organic tin(IV)-based metal halides via coordination structure modulation. Inorganic Chemistry Frontiers, [10.1039/D4QI01904K]
21. Zhaopeng Hu, Benteng Liu, Xin Jiang, Qiao Li, Hongda Meng, Yihu Song, Yongzhong Bao, Qiang Zheng. (2024) Regulating Vulcanization Kinetics with Deep Eutectic Solvents for Developing Greener Processing Technology of Thermoplastic Vulcanizates. ACS Sustainable Chemistry & Engineering, 12 (39): (14544-14552). [10.1021/acssuschemeng.4c06450]

参考文献

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17. Hongye Cheng, Guojin Zhang, Yaxi Zhang, Zhen Song, Zhiwen Qi. (2023) Solute structure effect on aromatics-alkanes extractive separation toward rational LCO upgrading. SEPARATION AND PURIFICATION TECHNOLOGY, 310 (123213). [10.1016/j.seppur.2023.123213]
18. Zhenyu Lu, Yufei Hu, Gongke Li, Ling Xia. (2022) Adamantane Three-Dimensional Porous Organic Framework as a Fluorescence Sensor for Rapid Determination of Tetracycline in Aquatic Products. Chemosensors, 10 (11): (457). [10.3390/chemosensors10110457]
19. Xueshan Sun, Xuezhen Wang, Yingli Wan, Yafei Guo, Tianlong Deng, Xiaoping Yu. (2023) Synthesis of functional ionic liquids with high extraction rate and electroconductivity for lithium-magnesium separation and metallic magnesium production from salt lake brine. CHEMICAL ENGINEERING JOURNAL, 452 (139610). [10.1016/j.cej.2022.139610]
20. Haolin Li, Lin Ma, Ping Wen, Yunyan Han, Rui Dong, Mingjin Fan. (2022) Molecular structure insight into the tribological behavior of sulfonate ionic liquids as lubricants for titanium alloys. JOURNAL OF MOLECULAR LIQUIDS, 357 (119082). [10.1016/j.molliq.2022.119082]
21. Zhen Ge, Hongye Cheng, Guojin Zhang, Linsheng Wang, Zhiwen Qi. (2022) Mechanism of Extractive Separation of Light Cycle Oil Using a Deep Eutectic Solvent Composed of Tetrabutylphosphonium Bromide and Levulinic Acid. ENERGY & FUELS, 36 (4): (1854–1862). [10.1021/acs.energyfuels.1c03856]
22. Yan Wang, Dong-Liang Zhong, Peter Englezos, Jin Yan, Bin-Bin Ge. (2020) Kinetic study of semiclathrate hydrates formed with CO2 in the presence of tetra-n-butyl ammonium bromide and tetra-n-butyl phosphonium bromide. ENERGY, 212 (118697). [10.1016/j.energy.2020.118697]
23. Zhiming Wu, Qian Zeng, Hongye Cheng, Lifang Chen, Zhiwen Qi. (2020) Extractive separation of tetralin-dodecane mixture using tetrabutylphosphonium bromide-based deep eutectic solvent. Chemical Engineering and Processing-Process Intensification, 149 (107822). [10.1016/j.cep.2020.107822]
24. Hongtao Cai, Ran Kou, Guangming Liu. (2019) Counterion-Tunable Thermosensitivity of Strong Polyelectrolyte Brushes. LANGMUIR, 35 (51): (16862–16868). [PMID:31774295] [10.1021/acs.langmuir.9b02982]
25. Yu-Mei Liu, Yan Zhou, Wen-Qiang Gong, Zhang-Min Li, Chao-Li Wang, Duan-Jian Tao. (2020) Highly efficient synthesis of 1-methoxy-2-propanol using ionic liquid catalysts in a micro-tubular circulating reactor. Green Energy & Environment, 5 (147). [10.1016/j.gee.2019.09.001]
26. Lei Liu, Xinyu Fu, Hongliang Zhang, Weiqing Ma, Lili Zhang, Yixin Zhang, Meng Liu, Kehan Liang, Senlin Hou, Aibing Chen. (2018) Luminogen-functionalized mesoporous SBA-15 for fluorescent detection of antibiotic cefalexin. JOURNAL OF MATERIALS RESEARCH, 33 (10): (1442-1448). [10.1557/jmr.2018.96]
27. Yalan Dai, Peiyi Wu. (2017) Toward the two-step microdynamic phase transition mechanism of an oligo(ethylene glycol)methacrylate-based copolymer with a LCST-type poly(ionic liquid) block. PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 19 (28): (18556-18564). [PMID:28686277] [10.1039/C7CP02942J]
28. Ge Wang, Peiyi Wu. (2016) Unusual Phase Transition Behavior of Poly(N-isopropylacrylamide)-co-Poly(tetrabutylphosphonium styrenesulfonate) in Water: Mild and Linear Changes in the Poly(N-isopropylacrylamide) Part. LANGMUIR, 32 (15): (3728–3736). [PMID:27022971] [10.1021/acs.langmuir.6b00392]
29. Ouyang Fan, Zhou Yan, Li Zhang-Min, Hu Na, Tao Duan-Jian. (2014) Tetrabutylphosphonium amino acid ionic liquids as efficient catalysts for solvent-free Knoevenagel condensation reactions. KOREAN JOURNAL OF CHEMICAL ENGINEERING, 31 (8): (1377-1383). [10.1007/s11814-014-0077-4]
30. Duan-Jian Tao, Fan Ouyang, Zhang-Min Li, Na Hu, Zhen Yang, Xiang-Shu Chen. (2013) Synthesis of Tetrabutylphosphonium Carboxylate Ionic Liquids and Its Catalytic Activities for the Alcoholysis Reaction of Propylene Oxide. INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 52 (48): (17111–17116). [10.1021/ie402250e]
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溶液计算器

摩尔浓度计算器

计算溶液所需的质量、体积或浓度。

质量

浓度

体积

分子量

g/mol

稀释计算器

计算配制储备溶液所需的稀释度。

浓度1（C1）

体积 1 (V1)

浓度 2 (C2)

体积 2 (V2)

复溶计算器

复溶计算器允许您快速计算试剂的体积，以复溶小瓶。只需输入试剂的质量和目标浓度，计算器将确定其余部分。

体积（添加到小瓶中）

质量（小瓶）

所需的复溶浓度