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醋酸钯

规格或纯度: 99.9% metals basis

CAS编号: 3375-31-3
分子式: C₄H₆O₄Pd
分子量: 224.51
Beilstein号: 6086766
EC号: 222-164-4
MDL号: MFCD00012453
PubChem编号: 167845

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货号 (SKU)	包装规格	是否现货	价格	数量
P111485-250mg	250mg	期货
P111485-1g	1g	现货
P111485-5g	5g	现货
P111485-10g	10g	期货
P111485-25g	25g	现货

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基本描述

别名	乙酸钯
英文别名	Palladium (II) acetate\|SR-01000389719\|EU-0040175\|BCP05504\|Palladium(II) acetate\|palladium-(II) acetate\|UNII-0LTG3460Y5\|Bis(acetato)palladium\|Acetic Acid Palladium(II) Salt\|AMY1789\|AC-677\|Diacetatopalladium\|Acetic acid palladium salt\|EINECS 222-164-4\|Aceti
规格或纯度	99.9% metals basis
英文名称	Palladium acetate
法律信息	Product of Umicore
运输条件	常规运输
产品介绍	Product class M-O, Homogeneous Catalysts, Acetate Ligands Reaction type Cross Coupling Reactions with Arenes, CH-Activation, Carbonylation, Mizoroki Heck Coupling Reaction, Sonogashira-Hagihara Coupling Reaction, Suzuki-Miyaura Coupling Reaction, Oxidation Chemical properties Chemical formula C12H18O12Pd3 Empirical formula [Pd(OAc)2]3 Molecular weight 673.53 Metal Pd Theoretical metal content 47 Physical state powder Color red brown Applications & references Synthesis of 2-(4-{2-[(2R)-2-Cyclopentyl-5-(5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidin-2-ylmethyl)-4-hydroxy-6-oxo-3,6-dihydro-2H-pyran-2-yl]-ethyl}-2-fluoro-phenyl)-2-methyl-propionitrile on multikilogram scale using a merging Heck coupling reaction. Compound is an inhibitor of the hepatitis C viral polymerase (HCVP) enzyme. Reference: Org. Proc. Res. Dev. 2006, 10, 814. (DOI: 10.1021/op0600761) Reductive carbonylation of aryl halides as an alternative and mild route for the introduction of aldehyde functionality, which is mostly desired for fine chemical and pharmaceutical intermediates to open up the wide range of further possible transformations. Reference: Org. Proc. Res. Dev. 2007, 11, 39. (DOI: 10.1021/op060193w) Synthesis of the pyrazolopyridinone-based p38 mitogen-activated protein kinase inhibitor including a Suzuki coupling reaction. p38 MAP kinases are intercellular serine/threonine kinases which certainly regulate the production and action of several pro-inflammatory mediators. They are also involved in disease states such as rheumatoid arthritis, Crohn’s diseases and psoriasis. Reference: Org. Proc. Res. Dev. 2011, 15, 31. (DOI: 10.1021/op100205s) Efficient hydroformylation of aryl triflates. Reference: Synthesis 1996, 470 (DOI: 10.1055/s-1996-4246) Deacetylation-Diazotation-Heck-Sequence: Carbon-Carbon bond formation with acetanilides as formal leaving groups Reference: Adv. Synth. Catal. 2013, 355, 463 (DOI: 10.1002/adsc.201200929) Deacetylation-Diazotation-Suzuki-Sequence: Carbon-Carbon bond formation with acetanilides as formal leaving groups. Reference: Adv. Synth. Catal. 2013, 355, 463 (DOI: 10.1002/adsc.201200929) Deacetylation-Diazotation-[2+2+1]-Cycloaddition: Reference: Adv. Synth. Catal. 2013, 355, 463 (DOI: 10.1002/adsc.201200929)

名称和标识符

EC号	222-164-4
IUPAC Name	palladium(2+);diacetate
INCHI	InChI=1S/2C2H4O2.Pd/c21-2(3)4;/h21H3,(H,3,4);/q;;+2/p-2
InChi Key	YJVFFLUZDVXJQI-UHFFFAOYSA-L
Canonical SMILES	CC(=O)[O-].CC(=O)[O-].[Pd+2]
Isomeric SMILES	CC(=O)[O-].CC(=O)[O-].[Pd+2]
WGK Germany	3
RTECS	AJ1900000
PubChem CID	167845
UN Number	3077
Packing Group	III
分子量	224.51
Beilstein号	6086766

化学和物理性质

熔点	216.3-223.7°C

安全和危险性（GHS）

象形图	Environmental Hazard Corrosive Harmful
信号词	Danger
危险声明	H302: Harmful if swallowed H318: Causes serious eye damage H317: May cause an allergic skin reaction H400: Very toxic to aquatic life H410: Very toxic to aquatic life with long lasting effects
预防措施声明	P261,P273,P280,P302+P352,P321,P501,P264,P270,P272,P333+P313,P362+P364,P391,P330,P264+P265,P301+P317,P305+P354+P338,P317
WGK Germany	3
RTECS	AJ1900000
Class	9
Merck Index	6991
个人防护装备	dust mask type N95 (US),Eyeshields,Gloves

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参考文献

1. Steven V Ley, Chandrashekar Ramarao, Richard S Gordon, Andrew B Holmes, Angus J Morrison, Ian F McConvey, Ian M Shirley, Stephen C Smith, Martin D Smith,. (2002-07-19) Polyurea-encapsulated palladium(II) acetate: a robust and recyclable catalyst for use in conventional and supercritical media.. Chemical communications (Cambridge, England), ((10)): ( 1134-1135 ). [PMID:12122701]
2. Ikuyo Kamiya,Etsuyo Nishinaka,Akiya Ogawa. (2005-01-18) Palladium(II) acetate in pyridine as an effective catalyst for highly regioselective hydroselenation of alkynes.. The Journal of organic chemistry, 70 ((2)): (696-698). [PMID:15651822]
3. Jinyue Ding,Taras Rybak,Dennis G Hall. (2014-11-19) Synthesis of chiral heterocycles by ligand-controlled regiodivergent and enantiospecific Suzuki Miyaura cross-coupling.. Nature communications, 5 (): (5474-5474). [PMID:25403650]
4. Mark S Chen,M Christina White. (2004-02-05) A sulfoxide-promoted, catalytic method for the regioselective synthesis of allylic acetates from monosubstituted olefins via C-H oxidation.. Journal of the American Chemical Society, 126 ((5)): (1346-1347). [PMID:14759185]
5. Matthew J Tredwell,Moises Gulias,Nadine Gaunt Bremeyer,Carin C C Johansson,Beatrice S L Collins,Matthew J Gaunt. (2011-01-27) Palladium(II)-catalyzed C-H bond arylation of electron-deficient arenes at room temperature.. Angewandte Chemie (International ed. in English), 50 ((5)): (1076-1079). [PMID:21268198]

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