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JOURNAL OF ORGANIC CHEMISTRY · 2021 · IF 4.354

Palladium-Catalyzed Stereoselective Difunctionalization of Bicyclic Alkenes with Organoammonium Salts and Organoboronic Compounds

Yuanyuan Tang,Kuan Liu,Jinjin Zhang,Long Liu,Tianzeng Huang,Chunya Li,Zhi Tang,Tieqiao Chen

A palladium-catalyzed difunctionalization of bicyclic alkenes with organoammonium salts and organoboronic compounds was reported. A wide range of functionalized cyclic products, including those bearing functional groups, were produced stereoselectively in good to excellent yields. The gram-scale experiment, one-pot operation, and synthetic application of β-borylated products further demonstrated the synthetic value of this new reaction in organic synthesis.

研究领域: 有机化学 · 合成化学

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JOURNAL OF ORGANIC CHEMISTRY · 2021 · IF 4.354

Copper-Catalyzed Cycloaddition of Heterobicyclic Alkenes with Diaryl Disulfides to Synthesize Dihydrobenzo[b]thiophene Derivatives

Qifu Lin,Wen Yang,Yongqi Yao,Yue Li,Lin Wang,Dingqiao Yang

A novel copper-catalyzed cycloaddition of diaryl disulfides to heterobicyclic alkenes has been developed. The C—S and C—C bonds can be formed simultaneously on the C═C bond of the olefins via a single-step cycloaddition to afford a series of 2,3-dihydrobenzo[b]thiophene derivatives. This reaction exhibits excellent diastereoselectivity and relatively broad substrate scope. Various functional groups attached to the substrates are tolerated in this protocol to give the corresponding exo adducts in moderate yields.

研究领域: 有机化学 · 合成化学

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