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A Strategy for Differentiating Oak Barrel Aged and Non-Oak Barrel Aged Wines by Using UHPLC–HRMS Combined with Chemometrics

Yi Lv,Feng-Lian Ma,Jia-Nan Wang,Yao Zhang,Yuan Jiang,Qian Ge,Yong-Jie Yu

The time involved and the high economic cost of using oak barrels to age wines have led to a significant price difference compared to non-oak barrel aged wines and may lead to some fraudulent sales in the market. In this study, an untargeted metabolomic strategy was developed to detect the metabolite composition of oak barrel aged and non-oak barrel aged wines in both positive and negative ion modes by using UHPLC–HRMS combined with the recently developed chemometric method AntDAS. The results of partial least squares discrimination analysis (PLS-DA) showed that the samples were characterized into two categories. Finally, 51 compounds were identified in positive ion mode, while 26 compounds were identified in negative ion mode. The results indicate that combining UHPLC–HRMS with AntDAS can reveal the material basis of wines and has excellent potential to differentiate between oak barrel aged and non-oak barrel aged wines.Keywords:oak barrel aged wines;UHPLC-HRMS;AntDAS;chemometrics