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ELECTROCHEMISTRY COMMUNICATIONS · 2012 · IF 4.859

Effect of Si, In and Ge doping on high ionic conductivity of Li7La3Zr2O12

Mian Huang,Alexandre Dumon,Ce-Wen Nan

The doping effect of Si, In and Ge in Li 7 La 3 Zr 2 O 12 (LLZ) as the solid electrolyte was studied via conventional solid-state reaction. The crystal structure, cross-sectional morphology, element distribution and conductivity were characterized for the undoped and doped LLZ ceramics. Our results showed that Si and In doping deteriorate electrical properties of LLZ as electrolyte, while Ge doping obviously improves properties. Ge might thus be a promising element for further increasing the ionic conductivity of LLZ ceramics.

研究领域: 材料科学 · 固态离子学

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SOLID STATE IONICS · 2013 · IF 2.046

High Li ion conductivity in strontium doped Li7La3Zr2O12 garnet

Alexandre Dumon,Mian Huang,Yang Shen,Ce-Wen Nan

Strontium doped lithium ion garnets Li 7 La 3 Zr 2 O 12 (LLZ) with 0.9 wt% to 8.4 wt% content of added Sr were synthesized via conventional solid-state reaction. X-ray diffraction patterns confirmed the cubic garnet structure of the sintered samples. A small amount of strontium was substituted to lanthanum in LLZ lattice. Further analysis showed SrCO 3 acted as a sintering aid for cubic LLZ ceramics and significantly increased the grain size of the sintered pellets. A conductivity of 2.10 × 10 − 4 S/cm at 297 K was obtained for the undoped LLZ. The total ionic conductivity reached a maximum of about 5 × 10 − 4 S/cm at 297 K with an activation energy of about 0.31 eV for 1.7 wt% Sr added LLZ sintered for 20–24 h in alumina crucible.

CAS / MDL: 554-13-2 1633-05-2

研究领域: 材料科学 · 固态离子学

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