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JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL · 2015 · IF 3.615

Efficient metal-free oxidation of ethylbenzene with molecular oxygen utilizing the synergistic combination of NHPI analogues

Qiming Zhao,Kexian Chen,Wensong Zhang,Jia Yao,Haoran Li

A metal- and initiator-free catalytic system comprising N -hydroxyquinolinimide (NHQI) and 4-carboxyl- N -hydroxyphthalimide (Car-NHPI) was developed for the oxidation of ethylbenzene using molecular oxygen as the terminal oxidant. The catalytic activity of Car-NHPI/NHQI catalytic system was higher than that of Car-NHPI or NHQI alone. The high catalytic performance of Car-NHPI/NHQI catalytic system could be attributed to the dual interactions of radical exchange and acid-base neutralization, which resulted in the increment of the conversion of ethylbenzene up to 70% and the selectivity of acetophenone up to 66% at 120 °C under 1 atm O 2 for 15 h.

CAS / MDL: 84-65-1 98-86-2 65-85-0 100-41-4 98-85-1 108-88-3

研究领域: 化学工程 · 环境科学

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