Synthesis of new rare earth containing ternary laminar Sc2PbC ceramic
In this paper, we combine rare earth element Sc and lead-containing MAX to predict a new ternary layered MAX phase Sc 2 PbC. Sc 2 PbC with a purity of 87.40 wt% was successfully synthesized by spark plasma sintering , and its crystal structure and atomic positions were obtained by X-ray diffraction (XRD). The Rietveld refinement results show that Sc 2 PbC belongs to a typical MAX phase P6 3 /mmc (No.194) space group with lattice parameters of a = 3.4003(7) Å and c = 14.7475(3) Å, where Sc atom is located at (1/3, 2/3, 0.57958), Pb atom is located at (1/3, 2/3, 1/4), and C atom is located at (0, 0, 0). At the same time, we observed the typical MAX phase layered microstructure in Sc 2 PbC bulk using a scanning electron microscope (SEM). In addition, the proportion of elements measured by energy dispersive spectroscopy (EDS) is within the allowable error range, which confirms that Sc 2 PbC is a new MAX phase compound.
危险品化学品经营许可证（带存储）