| 货号 (SKU) | 包装规格 | 是否现货 | 价格 | 数量 |
|---|---|---|---|---|
| BWY272961-1.2ml |
1.2ml |
现货  |
|
| 别名 | 哒螨灵,2-特丁基-5-(4-特丁苄基)硫代-4-氯-3(2氢)-哒嗪酮 | ||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 英文别名 | CAS-96489-71-3 | Pyramite | 2-t-butyl-5-(p-t-butylbenzylthio)-4-chloro-3(2H)-pyridazinone | AKOS015897404 | Pyridaben 10 microg/mL in Cyclohexane | MFCD00133627 | SMR000550490 | SR-01000789284 | Damanlin | tetraacetate | 3(2H)-Pyridazinone, 4-chloro-2-(1, | ||||||||||||||||
| 规格或纯度 | 1000μg/mL | ||||||||||||||||
| 英文名称 | Pyridaben in Methanol | ||||||||||||||||
| 储存温度 | 2-8°C储存,避光 | ||||||||||||||||
| 运输条件 | 冰袋运输 | ||||||||||||||||
| 产品介绍 |
本标准物质主要用于测量仪器校准、分析方法评价和质量控制，以及食品、卫生、环境和农业等领域相应成分含量测定与残留检测，也可作为标准储备溶液，通过逐级稀释配制成各种工作用标准溶液等。
样品制备
本标准物质采用纯度准确定值的哒螨灵纯品为原料，以农残级甲醇为溶剂，采用重量-容量法准确配制而成。 哒螨灵(别名：哒螨酮)，英文名称：Pyridaben，CAS：96489-71-3
溯源性及定值方法
本标准物质以配制值作为标准值，采用HPLC对本批次标准物质和质量控制对照样品进行比对，核验配制值。通过使用满足计量学特性要求的制备方法、测量方法和计量器具，保证标准物质的量值溯源性。
特性量值及不确定度
标准值的不确定度主要由原料纯度、称量、定容以及均匀性、稳定性等不确定度分量合成。
均匀性检验及稳定性考察
依据JJF1343-2012《标准物质定值的通用原则及统计学原理》，对分装后的样品进行随机抽样，对溶液浓度进行均匀性检验、稳定性考察。结果表明，本标准物质均匀性、稳定性良好。 本标准物质量值自定值日期起，有效期为24个月, 研制单位将继续跟踪监测该标准物质的稳定性，有效期内如发现量值变化，将及时通知用户。
包装、运输和贮存、使用及注意事项
1.包装：本标准物质采用硼硅酸盐玻璃安瓿瓶包装，约1.2mL/支，移取或稀释时请以移液管量取为准。 2.运输和贮存：冰袋运输，运输时应避免挤压、碰撞；冷藏和避光条件下贮存。 3.使用：启封前于室温（20±3℃）平衡，并充分摇匀。安瓿瓶一经打开，应立即使用，不可再次熔封后作为标准物质使用。 This standard substance is mainly used for measuring instrument calibration, analytical method evaluation and quality control, as well as the content determination and residue detection of corresponding components in the fields of food, hygiene, environment and agriculture. It can also be used as a standard stock solution and prepared into various types through successive dilutions. Standard solution for work, etc.
Sample Preparation
This standard material is made of pure pyridaben with accurate purity as raw material, pesticide residue methanol as solvent, and accurately prepared by the weight-volume method. Pyridaben (alias: pyridaben), English name: Pyridaben, CAS: 96489-71-3
Traceability and valuation method
This standard material uses the prepared value as the standard value, and uses HPLC to compare the batch of standard materials with the quality control control sample to verify the prepared value. Through the use of preparation methods, measurement methods and measuring instruments that meet the requirements of metrological characteristics, the traceability of the value of the reference material is guaranteed.
Characteristic value and uncertainty
The uncertainty of the standard value is mainly composed of raw material purity, weighing, constant volume, uniformity, stability and other uncertainty components.
Uniformity inspection and stability inspection
According to JJF1343-2012 "General Principles and Statistical Principles for Determining the Value of Standard Materials", random samples were taken of the subpackaged samples, and the uniformity and stability of the solution concentration were inspected. The results show that the standard material has good uniformity and stability. The quality value of this standard material is valid for 24 months from the date of setting the value. The development unit will continue to track and monitor the stability of the standard material. If there is any change in the value within the validity period, the user will be notified in time.
Packaging, transportation and storage, use and precautions
1. Packaging: This standard material is packaged in a borosilicate glass ampoule, about 1.2mL/piece. When pipetting or diluting, please refer to the pipette volume. 2. Transportation and storage: transport in ice bags, avoid squeezing and collision during transportation; store under refrigerated and dark conditions. 3. Use: Equilibrate at room temperature (20±3℃) before unsealing, and shake well. Once the ampoule is opened, it should be used immediately. It cannot be used as a standard substance after being sealed again. |
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| 作用机制 | Action Type | target ID | Target Name | Target Type | Target Organism | Binding Site Name | 参考文献 |
|---|
| EC号 | 405-700-3 |
|---|---|
| 分子类型 | 小分子 |
| IUPAC Name | 2-tert-butyl-5-[(4-tert-butylphenyl)methylsulfanyl]-4-chloropyridazin-3-one |
| INCHI | InChI=1S/C19H25ClN2OS/c1-18(2,3)14-9-7-13(8-10-14)12-24-15-11-21-22(19(4,5)6)17(23)16(15)20/h7-11H,12H2,1-6H3 |
| InChi Key | DWFZBUWUXWZWKD-UHFFFAOYSA-N |
| Canonical SMILES | CC(C)(C)C1=CC=C(C=C1)CSC2=C(C(=O)N(N=C2)C(C)(C)C)Cl |
| Isomeric SMILES | CC(C)(C)C1=CC=C(C=C1)CSC2=C(C(=O)N(N=C2)C(C)(C)C)Cl |
| WGK Germany | 3 |
| RTECS | UR6149000 |
| UN Number | 3077 |
| 分子量 | 364.93 |
| Beilstein号 | 7933972 |
| Reaxy-Rn | 7933972 |
| Reaxys-RN link address | https://www.reaxys.com/reaxys/secured/hopinto.do?context=S&query=IDE.XRN=7933972&ln= |
| 分子量 | 364.900 g/mol |
|---|---|
| XLogP3 | 5.200 |
| 氢键供体数Hydrogen Bond Donor Count | 0 |
| 氢键受体数Hydrogen Bond Acceptor Count | 3 |
| 可旋转键计数Rotatable Bond Count | 5 |
| 精确质量Exact Mass | 364.138 Da |
| 单同位素质量Monoisotopic Mass | 364.138 Da |
| 拓扑极表面积Topological Polar Surface Area | 58.000 Ų |
| 重原子数Heavy Atom Count | 24 |
| 形式电荷Formal Charge | 0 |
| 复杂度Complexity | 535.000 |
| 同位素原子数Isotope Atom Count | 0 |
| 定义的原子立体中心计数Defined Atom Stereocenter Count | 0 |
| 未定义的原子立体中心计数Undefined Atom Stereocenter Count | 0 |
| 定义的键立体中心计数Defined Bond Stereocenter Count | 0 |
| 未定义的键立体中心计数Undefined Bond Stereocenter Count | 0 |
| 所有立体化学键的总数The total count of all stereochemical bonds | 0 |
| 共价键合单元计数Covalently-Bonded Unit Count | 1 |
| 象形图 | GHS06, GHS09 |
|---|---|
| 信号词 | Danger |
| 危险声明 |
H301: 吞咽会中毒 H331: 吸入会中毒 H400: 对水生生物有剧毒 H410: 对水生生物有剧毒并具有长期持续影响 |
| 预防措施声明 |
P261: 避免吸入灰尘/烟雾/气体/雾/蒸汽/喷雾 P273: 避免释放到环境中。 P321: 特殊处理（请参阅此标签上的...）。 P405: 密闭存放 P501: 将内容物/容器处理到。。。 P264: 处理后要彻底洗手。 P271: 仅在室外或通风良好的地方使用。 P270: 使用本产品时，请勿进食、饮水或吸烟。 P304+P340: 如误吸入：将人转移到空气新鲜处，保持呼吸舒适体位。 P403+P233: 存放在通风良好的地方。保持容器密闭。 P391: 收集溢出物 P330: 漱口 P301+P316: 如果吞咽：立即寻求紧急医疗救助。 P316: 立即寻求紧急医疗救助。 |
| WGK Germany | 3 |
| RTECS | UR6149000 |
| Reaxy-Rn | 7933972 |
| Reaxys-RN link address | https://www.reaxys.com/reaxys/secured/hopinto.do?context=S&query=IDE.XRN=7933972&ln= |
| 个人防护装备 | Eyeshields,Faceshields,Gloves,type P2 (EN 143) respirator cartridges |
| Concentration(w/v) | 980-1020(μg/ml) |
|---|---|
| Appearance(BWY272961) | Colourless Transparent Liquid |
| 1. Mei-ting Guo, Ting-feng Shi, Run Tian, Ping Lu, Ting-tiao Pan. (2024) Adsorption behavior of pyridaben on silver surface and detection of pyridaben residues in apple. MICROCHEMICAL JOURNAL, 197 (15): (109635). [PMID:1541829] [10.1016/j.microc.2023.109635] |
| 2. Jiaxuan Fan, Jing Li, Wenfeng Zhou, Haixiang Gao, Runhua Lu. (2023) A low-cost, efficient and selective detection method of acaricide residues: Adsorption study. MICROCHEMICAL JOURNAL, 186 (108325). [10.1016/j.microc.2022.108325] |
| 3. Gu Yu-Xin, Yan Tian-Ci, Yue Zi-Xuan, Li Min-Hui, Zheng Hui, Wang Shu-Ling, Cao Jun. (2022) Dispersive Micro-solid-Phase Extraction of Acaricides from Fruit Juice and Functional Food Using Cucurbituril as Sorbent. Food Analytical Methods, 15 (5): (1356-1367). [10.1007/s12161-021-02209-8] |
| 4. Ning Shen, Yao Li, Kipchoge Leviticus, Xiao Li Chang, Tao Tang, Li Cui, Zhao Jun Han, Chun Qing Zhao. (2021) Effect of broflanilide on the phytophagous mite Tetranychus urticae and the predatory mite Typhlodromips swirskii. PEST MANAGEMENT SCIENCE, 77 (6): (2964-2970). [PMID:33624401] [10.1002/ps.6335] |
| 5. Xiao-Chun Ma, Zong-Qin Ma, Meng-Xin Zhao, Ying-Hui Wang, Yuan Peng, Xin Guo, Fang-Huan Wang, Zhe Meng, Hao-Bo Zheng. (2021) Facile synthesis of magnetic molybdenum disulfide@graphene nanocomposite with amphiphilic properties and its application in solid-phase extraction for a wide polarity of insecticides in wolfberry samples. Analytical Methods, 13 (5): (672-684). [PMID:33475104] [10.1039/D0AY01939A] |
| 6. Kipchoge Leviticus, Li Cui, Han Ling, Zhong-Qiang Jia, Qiu-Tang Huang, Zhao-Jun Han, Chun-Qing Zhao, Lu Xu. (2019) Lethal and sublethal effects of fluralaner on the two-spotted spider mites, Tetranychus urticae Koch (Acari: Tetranychidae). PEST MANAGEMENT SCIENCE, 76 (3): (888-893). [PMID:31429178] [10.1002/ps.5593] |
| 7. Weiping Wang, Hualing Zhu, Shumin Cui, Jigen Miao, Jianrong Chen. (2014) Ultrasound-assisted dispersive liquid–liquid microextraction based on solidification of floating organic droplets coupled with gas chromatography for the determination of pesticide residues in water samples. Analytical Methods, 6 (10): (3388-3394). [10.1039/C3AY42331J] |
| 8. Bing Peng, Xiaoling Yang, Jiaheng Zhang, Fengpei Du, Wenfeng Zhou, Haixiang Gao, Runhua Lu. (2013) Comparison of two ultrasound-enhanced microextractions combined with HPLC for determining acaricides in water. JOURNAL OF SEPARATION SCIENCE, 36 (13): (2196-2202). [PMID:23596154] [10.1002/jssc.201300283] |
| 9. Cui Shumin, Chen Qianxia, Wang Weiping, Miao Jigen, Wang Aijun, Chen Jianrong. (2013) Ultra-Preconcentration and Determination of Multiple Pesticide Residues in Water Samples Using Ultrasound-Assisted Dispersive Liquid–Liquid Microextraction and GC-FID. CHROMATOGRAPHIA, 76 (11): (671-678). [10.1007/s10337-013-2441-7] |
| 1. Mei-ting Guo, Ting-feng Shi, Run Tian, Ping Lu, Ting-tiao Pan. (2024) Adsorption behavior of pyridaben on silver surface and detection of pyridaben residues in apple. MICROCHEMICAL JOURNAL, 197 (15): (109635). [PMID:1541829] [10.1016/j.microc.2023.109635] |
| 2. Jiaxuan Fan, Jing Li, Wenfeng Zhou, Haixiang Gao, Runhua Lu. (2023) A low-cost, efficient and selective detection method of acaricide residues: Adsorption study. MICROCHEMICAL JOURNAL, 186 (108325). [10.1016/j.microc.2022.108325] |
| 3. Gu Yu-Xin, Yan Tian-Ci, Yue Zi-Xuan, Li Min-Hui, Zheng Hui, Wang Shu-Ling, Cao Jun. (2022) Dispersive Micro-solid-Phase Extraction of Acaricides from Fruit Juice and Functional Food Using Cucurbituril as Sorbent. Food Analytical Methods, 15 (5): (1356-1367). [10.1007/s12161-021-02209-8] |
| 4. Ning Shen, Yao Li, Kipchoge Leviticus, Xiao Li Chang, Tao Tang, Li Cui, Zhao Jun Han, Chun Qing Zhao. (2021) Effect of broflanilide on the phytophagous mite Tetranychus urticae and the predatory mite Typhlodromips swirskii. PEST MANAGEMENT SCIENCE, 77 (6): (2964-2970). [PMID:33624401] [10.1002/ps.6335] |
| 5. Xiao-Chun Ma, Zong-Qin Ma, Meng-Xin Zhao, Ying-Hui Wang, Yuan Peng, Xin Guo, Fang-Huan Wang, Zhe Meng, Hao-Bo Zheng. (2021) Facile synthesis of magnetic molybdenum disulfide@graphene nanocomposite with amphiphilic properties and its application in solid-phase extraction for a wide polarity of insecticides in wolfberry samples. Analytical Methods, 13 (5): (672-684). [PMID:33475104] [10.1039/D0AY01939A] |
| 6. Kipchoge Leviticus, Li Cui, Han Ling, Zhong-Qiang Jia, Qiu-Tang Huang, Zhao-Jun Han, Chun-Qing Zhao, Lu Xu. (2019) Lethal and sublethal effects of fluralaner on the two-spotted spider mites, Tetranychus urticae Koch (Acari: Tetranychidae). PEST MANAGEMENT SCIENCE, 76 (3): (888-893). [PMID:31429178] [10.1002/ps.5593] |
| 7. Weiping Wang, Hualing Zhu, Shumin Cui, Jigen Miao, Jianrong Chen. (2014) Ultrasound-assisted dispersive liquid–liquid microextraction based on solidification of floating organic droplets coupled with gas chromatography for the determination of pesticide residues in water samples. Analytical Methods, 6 (10): (3388-3394). [10.1039/C3AY42331J] |
| 8. Bing Peng, Xiaoling Yang, Jiaheng Zhang, Fengpei Du, Wenfeng Zhou, Haixiang Gao, Runhua Lu. (2013) Comparison of two ultrasound-enhanced microextractions combined with HPLC for determining acaricides in water. JOURNAL OF SEPARATION SCIENCE, 36 (13): (2196-2202). [PMID:23596154] [10.1002/jssc.201300283] |
| 9. Cui Shumin, Chen Qianxia, Wang Weiping, Miao Jigen, Wang Aijun, Chen Jianrong. (2013) Ultra-Preconcentration and Determination of Multiple Pesticide Residues in Water Samples Using Ultrasound-Assisted Dispersive Liquid–Liquid Microextraction and GC-FID. CHROMATOGRAPHIA, 76 (11): (671-678). [10.1007/s10337-013-2441-7] |
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