| 货号 (SKU) | 包装规格 | 是否现货 | 价格 | 数量 |
|---|---|---|---|---|
| BWY272963-1.2ml |
1.2ml |
现货  |
|
| 别名 | 速保利 | ||||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 英文别名 | 1H-1,2,4-Triazole-1-ethanol, beta-((2,4-dichlorophenyl)methylene)-alpha-(1,1-dimethylethyl)-, (E)- | NCGC00168303-01 | (E)-1-(2,4-dichlorophenyl)-2-(1,2,4-triazol-1-yl)-4,4-dimethyl-1-penten-3-ol | Q27157324 | Spotless, Mixor | A838806 | p-Mentha-1,3,5,8- | ||||||||||||||||
| 规格或纯度 | 100μg/mL in Methanol | ||||||||||||||||
| 英文名称 | Diniconazole in Methanol | ||||||||||||||||
| 储存温度 | 2-8°C储存,避光 | ||||||||||||||||
| 运输条件 | 冰袋运输 | ||||||||||||||||
| 产品介绍 |
本标准物质主要用于测量仪器校准,分析方法评价和质量控制,以及食品,卫生,环境和农业等领域相应成分含量测定与残留检测,也可用于量值溯源或作为标准储备溶液,通过逐级稀释配制成各种工作用标准溶液等。
样品制备
本标准物质采用纯度准确定值的烯唑醇纯品为原料,以HPLC级甲醇为溶剂,采用重量-容量法准确配制而成。
本标准物质以配制值作为标准值,采用HPLC-MS对本批次标准物质和质量控制对照样品进行比对,核验配制值。通过使用满足计量学特性要求的制备方法,测量方法和计量器具,保证标准物质的量值溯源性。
特性量值及不确定度
均匀性检验及稳定性考察
依据JJF1343-2012[标准物质定值的通用原则及统计学原理],对分装后的样品进行随机抽样,对溶液浓度进行均匀性检验,稳定性考察。结果表明,本标准物质均匀性,稳定性良好。
包装、运输和贮存、使用及注意事项
1.包装: 本标准物质采用硼硅酸盐玻璃安瓿瓶包装,约1.2mL/支,移取或稀释时请以移液管量取为准。 This standard substance is mainly used for measuring instrument calibration, analysis method evaluation and quality control, as well as the content determination and residue detection of corresponding components in the fields of food, hygiene, environment and agriculture. It can also be used for value traceability or as a standard stock solution. Dilute and prepare various standard solutions for work.
Sample Preparation
This standard material is made of pure diniconazole with accurate purity as the raw material, HPLC grade methanol as the solvent, and accurately prepared by the weight-volume method.
Traceability and valuation method
This standard material uses the prepared value as the standard value, and uses HPLC-MS to compare the batch of standard materials and quality control control samples to verify the prepared value. Through the use of preparation methods, measurement methods and measuring instruments that meet the requirements of metrological characteristics, the traceability of the value of the reference material is guaranteed.
Characteristic value and uncertainty
The uncertainty of the standard value is mainly composed of raw material purity, weighing, constant volume, uniformity, stability and other uncertainty components.
Uniformity inspection and stability inspection
According to JJF1343-2012 [General Principles and Statistical Principles for Determining Standard Material Values], the samples after subpackage are randomly sampled, the solution concentration is tested for uniformity and stability. The results show that the standard material has good uniformity and stability. The quality value of this standard material is valid for 24 months from the date of setting the value. The development unit will continue to track and monitor the stability of the standard material. If the value changes within the validity period, the user will be notified in time.
Packaging, transportation and storage, use and precautions
1. Packaging: This standard material is packaged in a borosilicate glass ampoule, about 1.2mL/piece, please refer to the pipette volume when pipetting or diluting. 2. Transportation and storage: ice bag transportation, avoid squeezing and collision during transportation; store under refrigerated and dark conditions. 3. Use: Before unsealing, equilibrate at room temperature (20±3)℃ and shake well. Once the ampoule is opened, it should be used immediately. It cannot be used as a standard substance after being sealed again. |
| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 活性类型 | Relation | Activity value | Units | Action Type | Journal | PubMed Id | doi | Assay Aladdin ID |
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| 作用机制 | Action Type | target ID | Target Name | Target Type | Target Organism | Binding Site Name | 参考文献 |
|---|
| 分子类型 | 小分子 |
|---|---|
| IUPAC Name | (E)-1-(2,4-dichlorophenyl)-4,4-dimethyl-2-(1,2,4-triazol-1-yl)pent-1-en-3-ol |
| INCHI | InChI=1S/C15H17Cl2N3O/c1-15(2,3)14(21)13(20-9-18-8-19-20)6-10-4-5-11(16)7-12(10)17/h4-9,14,21H,1-3H3/b13-6+ |
| InChi Key | FBOUIAKEJMZPQG-AWNIVKPZSA-N |
| Canonical SMILES | CC(C)(C)C(C(=CC1=C(C=C(C=C1)Cl)Cl)N2C=NC=N2)O |
| Isomeric SMILES | CC(C)(C)C(/C(=C\C1=C(C=C(C=C1)Cl)Cl)/N2C=NC=N2)O |
| 分子量 | 326.22 |
| Beilstein号 | 9202976 |
| Reaxy-Rn | 8265704 |
| Reaxys-RN link address | https://www.reaxys.com/reaxys/secured/hopinto.do?context=S&query=IDE.XRN=8265704&ln= |
| 熔点 | 134-156°C |
|---|---|
| 分子量 | 326.200 g/mol |
| XLogP3 | 4.200 |
| 氢键供体数Hydrogen Bond Donor Count | 1 |
| 氢键受体数Hydrogen Bond Acceptor Count | 3 |
| 可旋转键计数Rotatable Bond Count | 4 |
| 精确质量Exact Mass | 325.075 Da |
| 单同位素质量Monoisotopic Mass | 325.075 Da |
| 拓扑极表面积Topological Polar Surface Area | 50.900 Ų |
| 重原子数Heavy Atom Count | 21 |
| 形式电荷Formal Charge | 0 |
| 复杂度Complexity | 384.000 |
| 同位素原子数Isotope Atom Count | 0 |
| 定义的原子立体中心计数Defined Atom Stereocenter Count | 0 |
| 未定义的原子立体中心计数Undefined Atom Stereocenter Count | 1 |
| 定义的键立体中心计数Defined Bond Stereocenter Count | 1 |
| 未定义的键立体中心计数Undefined Bond Stereocenter Count | 0 |
| 所有立体化学键的总数The total count of all stereochemical bonds | 1 |
| 共价键合单元计数Covalently-Bonded Unit Count | 1 |
| 象形图 | GHS09, GHS07 |
|---|---|
| 信号词 | Warning |
| 危险声明 |
H302: 吞食有害 H400: 对水生生物有剧毒 H410: 对水生生物有剧毒并具有长期持续影响 |
| 预防措施声明 |
P273: 避免释放到环境中。 P501: 将内容物/容器处理到。。。 P264: 处理后要彻底洗手。 P270: 使用本产品时，请勿进食、饮水或吸烟。 P391: 收集溢出物 P330: 漱口 P301+P317: 如果被吞咽：请寻求医疗帮助。 |
| Reaxy-Rn | 8265704 |
| Reaxys-RN link address | https://www.reaxys.com/reaxys/secured/hopinto.do?context=S&query=IDE.XRN=8265704&ln= |
| Appearance(BWY272963) | Colorless Transparent Liquid |
|---|---|
| Solvent(Methanol) | Conform |
| Concentration(w/v) | 98-102（μg/ml） |
| 1. Xiaoyu Yang. (2023) Simultaneous Enantioseparation of Three Chiral Antifungal Pesticides by Hydroxypropyl-γ-CD-Modified Micellar Electrokinetic Chromatography. Journal of Analytical Methods in Chemistry, 2023 (21): (9993526). [PMID:37849914] [10.1155/2023/9993526] |
| 2. Ruiyu Fu, Tingze Ren, Yanhui Zhang, Qingxin Lu, Xiaoli Guo, Xin Di. (2023) Hexafluoroisopropanol-based supramolecular solvent for liquid phase microextraction of triazole fungicides in drinking water and beverages. MICROCHEMICAL JOURNAL, 191 (108842). [10.1016/j.microc.2023.108842] |
| 3. Yang Liu, Liqiang Liu, Xinxin Xu, Chuanlai Xu, Liguang Xu. (2023) Gold nanoparticle-based lateral flow immunoassay for the rapid detection of flutriafol residues in food. Materials Chemistry Frontiers, 7 (5): (955-963). [10.1039/D2QM01231F] |
| 4. Wenhui Li, Ying Gu, Zikun Liu, Rimao Hua, Xiangwei Wu, Jiaying Xue. (2022) Development of a polyurethane-coated thin film solid phase microextraction device for multi-residue monitoring of pesticides in fruit and tea beverages. JOURNAL OF SEPARATION SCIENCE, 46 (2): (2200661). [PMID:36373185] [10.1002/jssc.202200661] |
| 5. Min Sun, Haili Sun, Juanjuan Feng, Jiaqing Feng, Jing Fan, Mingxia Sun, Yang Feng. (2022) Carbonized metal-organic framework-74/carbon aerogel composites for the efficient extraction of triazole fungicides from fruits and vegetables. JOURNAL OF CHROMATOGRAPHY A, 1683 (463552). [PMID:36219967] [10.1016/j.chroma.2022.463552] |
| 6. Haili Sun, Juanjuan Feng, Jiaqing Feng, Mingxia Sun, Yang Feng, Min Sun. (2022) Carbon aerogels derived from waste paper for pipette-tip solid-phase extraction of triazole fungicides in tomato, apple and pear. FOOD CHEMISTRY, 395 (133633). [PMID:35816989] [10.1016/j.foodchem.2022.133633] |
| 7. Liu Yang, Xu Xinxin, Liu Liqiang, Xu Liguang, Kuang Hua, Xu Chuanlai. (2022) Gold-based lateral-flow strip for the detection of penconazole in watermelon and cucumber samples. Food Quality and Safety, 6 [10.1093/fqsafe/fyac007] |
| 8. Jian Zhu, Shuang Zhang, Guo-jun Weng, Jian-jun Li, Jun-wu Zhao. (2021) Spiky yolk-shell AuAg bimetallic nanorods with uniform interior gap for the SERS detection of thiram residues in fruit juice. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 262 (120108). [PMID:34198118] [10.1016/j.saa.2021.120108] |
| 9. Suling Zhang, Ziluo Hua, Hongting Zhao, Weixuan Yao, Yuanzhao Wu, Defeng Fu, Jiancong Sun. (2021) Defective Zr-based metal–organic frameworks as sorbent for the determination of fungicides in environmental water samples by rapid dispersive micro-solid-phase extraction coupled to liquid chromatography/mass spectrometry. JOURNAL OF SEPARATION SCIENCE, 44 (10): (2113-2120). [PMID:33721403] [10.1002/jssc.202001240] |
| 10. Weixuan Yao, Zhefeng Fan, Suling Zhang. (2019) Preparation of metal-organic framework UiO-66-incorporated polymer monolith for the extraction of trace levels of fungicides in environmental water and soil samples. JOURNAL OF SEPARATION SCIENCE, 42 (16): (2679-2686). [PMID:31177628] [10.1002/jssc.201900168] |
| 11. Xiao-jing Mao, Jing Li, Dan Liu, Ting Qiao, Liyun Ma, Xiao Sun, Li Xu, Zhi-guo Shi. (2018) Flow-through silica: A potential matrix for fast chromatographic enantioseparation with high enantioselectivity. TALANTA, 178 (583). [PMID:29136866] [10.1016/j.talanta.2017.09.093] |
| 12. Shuaihua Zhang, Qian Yang, Wenchang Wang, Chun Wang, Zhi Wang. (2016) Covalent Bonding of Metal–Organic Framework-5/Graphene Oxide Hybrid Composite to Stainless Steel Fiber for Solid-Phase Microextraction of Triazole Fungicides from Fruit and Vegetable Samples. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 64 (13): (2792–2801). [PMID:26998567] [10.1021/acs.jafc.5b05831] |
| 13. Xiaofei Han,Jia Chen,Zhan Li,Kaijun Quan,Hongdeng Qiu. (2020-09-07) Magnetic solid-phase extraction of triazole fungicides based on magnetic porous carbon prepared by combustion combined with solvothermal method.. Analytica chimica acta, 1129 (85-97). [PMID:32891394] |
| 1. Xiaoyu Yang. (2023) Simultaneous Enantioseparation of Three Chiral Antifungal Pesticides by Hydroxypropyl-γ-CD-Modified Micellar Electrokinetic Chromatography. Journal of Analytical Methods in Chemistry, 2023 (21): (9993526). [PMID:37849914] [10.1155/2023/9993526] |
| 2. Ruiyu Fu, Tingze Ren, Yanhui Zhang, Qingxin Lu, Xiaoli Guo, Xin Di. (2023) Hexafluoroisopropanol-based supramolecular solvent for liquid phase microextraction of triazole fungicides in drinking water and beverages. MICROCHEMICAL JOURNAL, 191 (108842). [10.1016/j.microc.2023.108842] |
| 3. Yang Liu, Liqiang Liu, Xinxin Xu, Chuanlai Xu, Liguang Xu. (2023) Gold nanoparticle-based lateral flow immunoassay for the rapid detection of flutriafol residues in food. Materials Chemistry Frontiers, 7 (5): (955-963). [10.1039/D2QM01231F] |
| 4. Wenhui Li, Ying Gu, Zikun Liu, Rimao Hua, Xiangwei Wu, Jiaying Xue. (2022) Development of a polyurethane-coated thin film solid phase microextraction device for multi-residue monitoring of pesticides in fruit and tea beverages. JOURNAL OF SEPARATION SCIENCE, 46 (2): (2200661). [PMID:36373185] [10.1002/jssc.202200661] |
| 5. Min Sun, Haili Sun, Juanjuan Feng, Jiaqing Feng, Jing Fan, Mingxia Sun, Yang Feng. (2022) Carbonized metal-organic framework-74/carbon aerogel composites for the efficient extraction of triazole fungicides from fruits and vegetables. JOURNAL OF CHROMATOGRAPHY A, 1683 (463552). [PMID:36219967] [10.1016/j.chroma.2022.463552] |
| 6. Haili Sun, Juanjuan Feng, Jiaqing Feng, Mingxia Sun, Yang Feng, Min Sun. (2022) Carbon aerogels derived from waste paper for pipette-tip solid-phase extraction of triazole fungicides in tomato, apple and pear. FOOD CHEMISTRY, 395 (133633). [PMID:35816989] [10.1016/j.foodchem.2022.133633] |
| 7. Liu Yang, Xu Xinxin, Liu Liqiang, Xu Liguang, Kuang Hua, Xu Chuanlai. (2022) Gold-based lateral-flow strip for the detection of penconazole in watermelon and cucumber samples. Food Quality and Safety, 6 [10.1093/fqsafe/fyac007] |
| 8. Jian Zhu, Shuang Zhang, Guo-jun Weng, Jian-jun Li, Jun-wu Zhao. (2021) Spiky yolk-shell AuAg bimetallic nanorods with uniform interior gap for the SERS detection of thiram residues in fruit juice. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 262 (120108). [PMID:34198118] [10.1016/j.saa.2021.120108] |
| 9. Suling Zhang, Ziluo Hua, Hongting Zhao, Weixuan Yao, Yuanzhao Wu, Defeng Fu, Jiancong Sun. (2021) Defective Zr-based metal–organic frameworks as sorbent for the determination of fungicides in environmental water samples by rapid dispersive micro-solid-phase extraction coupled to liquid chromatography/mass spectrometry. JOURNAL OF SEPARATION SCIENCE, 44 (10): (2113-2120). [PMID:33721403] [10.1002/jssc.202001240] |
| 10. Weixuan Yao, Zhefeng Fan, Suling Zhang. (2019) Preparation of metal-organic framework UiO-66-incorporated polymer monolith for the extraction of trace levels of fungicides in environmental water and soil samples. JOURNAL OF SEPARATION SCIENCE, 42 (16): (2679-2686). [PMID:31177628] [10.1002/jssc.201900168] |
| 11. Xiao-jing Mao, Jing Li, Dan Liu, Ting Qiao, Liyun Ma, Xiao Sun, Li Xu, Zhi-guo Shi. (2018) Flow-through silica: A potential matrix for fast chromatographic enantioseparation with high enantioselectivity. TALANTA, 178 (583). [PMID:29136866] [10.1016/j.talanta.2017.09.093] |
| 12. Shuaihua Zhang, Qian Yang, Wenchang Wang, Chun Wang, Zhi Wang. (2016) Covalent Bonding of Metal–Organic Framework-5/Graphene Oxide Hybrid Composite to Stainless Steel Fiber for Solid-Phase Microextraction of Triazole Fungicides from Fruit and Vegetable Samples. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 64 (13): (2792–2801). [PMID:26998567] [10.1021/acs.jafc.5b05831] |
| 13. Xiaofei Han,Jia Chen,Zhan Li,Kaijun Quan,Hongdeng Qiu. (2020-09-07) Magnetic solid-phase extraction of triazole fungicides based on magnetic porous carbon prepared by combustion combined with solvothermal method.. Analytica chimica acta, 1129 (85-97). [PMID:32891394] |
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