Rapid and facile preparation of NiFe-layered double hydroxide nanosheets as self-supported electrode for glucose detection in drink sample

Layered double hydroxides have been widely used for electrochemical glucose detection due to their layered structure with more active sites, but they suffer from lower electrical conductivity and long-time hydrothermal preparation. In this paper, NiFe-layered double hydroxide nanosheets supported on nickel foam (NiFe-LDH NSs/NF) was prepared using an ultrafast and facile method via in-situ corroding foam nickel in FeCl 3 solution under room temperature, and the whole synthetic process can be accomplished within several minutes. The as-fabricated NiFe-LDH NSs/NF shows significant catalytic activity in the glucose oxidation, showing its great promise in glucose detection. As a self-supported electrode, NiFe-LDH NSs/NF is favorable for glucose detection, with a sensitivity of 9.79 and 3.29 mA mM −1  cm −2 within the linear range of 0.001 to 1.16 mM and 1.16 to 4.67 mM, respectively. Moreover, NiFe-LDH NSs/NF is also selective and reliable towards glucose detection in drink sample.