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Fabrication and characterizations of 8.7 mol% Y2O3-ZrO2 transparent ceramics using co-precipitated nanopowders

Journal 2019 · IF 4.539 · 发表于 2019 年 7 月 2 日
作者: Qiang Liu,Penghui Chen,Nan Jiang,Xing Zhang,Xiaoying Li,Sha Su,Zewang Hu,Haohong Chen,Tengfei Xie,Jiang Li
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摘要

8.7 mol% Y 2 O 3 -ZrO 2 (Y 0.16 Zr 0.84 O 1.92 ) precursor was synthesized by the co-precipitation method using ammonia as the precipitant. The Y 0.16 Zr 0.84 O 1.92 powders calcined at 800 °C show a pure c-ZrO 2 phase. The average crystallite size of the powders is 12.4 nm and weakly agglomerated to an average particle size of 15.5 nm. Y 0.16 Zr 0.84 O 1.92 transparent ceramics were then successfully fabricated by pre-sintering at 1350 °C for 2 h and HIP post-treatment at 1750 °C for 1 h under 200 MPa without sintering additives. The in-line transmittance of Y 0.16 Zr 0.84 O 1.92 ceramics (1 mm thick) exceeds 50.3% in the region of 400–850 nm, reaching about 65.3% at 800 nm.

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