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Preparation and properties of mullite-bonded porous fibrous mullite ceramics by an epoxy resin gel-casting process

Journal 2017 · IF 2.986 · 发表于 2017 年 1 月 12 日
作者: Lei Yuan,Beiyue Ma,Qiang Zhu,Xiaodong Zhang,Han Zhang,Jingkun Yu
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摘要

Porous fibrous mullite ceramics with a narrow range of pore size distribution have been successfully prepared utilizing a near net-shape epoxy resin gel-casting process by using mullite fibers, Al 2 O 3 and SiC as raw materials. The effects of sintering temperatures , different amounts of fibers and Y 2 O 3 additive on the phase compositions, linear shrinkage, apparent porosity, bulk density, microstructure, compressive strength and thermal conductivity were investigated. The results indicated that mullite-bonded among fibers were formed in the porous fibrous mullite ceramics with a bird nest pore structure . After determining the sintering temperatures and the amount of fibers, the tailored porous fibrous mullite ceramics had a low linear shrinkage (1.36–3.08%), a high apparent porosity (61.1–71.7%), a relatively high compressive strength (4.4–7.6   MPa), a low thermal conductivity (0.378–0.467   W/m   K) and a narrow range of pore size distribution (around 5   µm). The excellent properties will enable the porous ceramics as a promising candidate for the applications of hot gas filters, thermal insulation materials at high temperatures.

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