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Granulation of Y2O3 powders by a vibration method for the preparation of transparent ceramics

Journal 2016 · IF 3.289 · 6(107): 105755-105760 · 发表于 2016 年 10 月 31 日
作者: Xiaokai Li,Yangyang Xu,Xiaojian Mao,Qiangqiang Zhu,Minghui Feng,Benxue Jiang,Long Zhang
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摘要

A modified vibrating screen method was employed to prepare granulated Y2O3 powders, which were used to fabricate transparent ceramics. The granulation process was carried out with yttrium-stabilized zirconia balls (5 mm in diameter) in a 200-mesh screen, which was vibrated by a Heidolph shaker. After passage through the vibrating screen, the sub-micron Y2O3 particles were converted into large granules and collected in the bottom chamber of the sieve. Compared with the original powders, the granulated powders had a smaller repose angle of 34.09° and larger apparent and tap densities with sharp rises of 50.54 and 32.07%, respectively, indicating a good flowability and filling properties. A high transmittance of 82% at 2500 nm was achieved for ceramics prepared using the granulated powders by vacuum sintering and hot isostatic pressing (HIP).