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Fabrication of complex-shaped zirconia ceramic parts via a DLP- stereolithography-based 3D printing method

Journal 2017 · IF 2.986 · 44(3): 3412-3416 · 发表于 2017 年 11 月 21 日
作者: Rongxuan He,Wei Liu,Ziwei Wu,Di An,Meipeng Huang,Haidong Wu,Qiangguo Jiang,Xuanrong Ji,Shanghua Wu,Zhipeng Xie
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摘要

In this work, a stereolithography-based method of 3D printing was successfully used to fabricate a complex-shaped triangular zirconia cutting tool with a tool withdrawal groove and a honeycomb ceramic component. The sintered bodies displayed significant shrinkage after sintering, with the maximum shrinkage being 35.26%. The XRD pattern indicated that the crystalline phase of the parts was the t-ZrO 2 phase, while SEM characterization revealed that the sintered bodies were composed of densely packed submicron-grade grains, without any discernible pores. The density of the parts was measured as 97.14% via Archimedes’ water displacement method, which is consistent with the results of SEM characterization. Additionally, the measured Vickers hardness and fracture toughness of the fabricated parts were 13.0597   GPa and 6.0380   MPa   m 1/2 , respectively. These values are close to the structural properties of common zirconia ceramics prepared by conventional approaches. Hence, a novel DLP-stereolithography-based 3D printing process for the fabrication of complex and dense zirconia ceramic parts has been proposed in this work.